串联质谱在农残分析应用研究进展
Journal: Ecological Environment and Protection DOI: 10.12238/eep.v7i5.2053
Abstract
本文针对国内外串联质谱农残分析进行了应用研究,重点在三重四级杆串联质谱、离子阱质谱技术等方面进行了对比,最后提出了目前我国农残分析的串联质谱应用现状。
Keywords
串联质谱；农残分析；三重四级杆串联质谱；离子阱质谱
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[3] Dickerson AS,Wu AC,Liew Z,Weisskopf M.(2020)A Scoping Review of Non-Occupation-al Exposures to Environmental Poll utants and Adult Depression, Anxiety, and Suicide. Curr Envi ron Health Rep,7,256-271.
[4] 孔祥虹.固相微萃取-气相色谱法测定浓缩汁中的8种有机磷农药残留[J].食品科学,2009,30(2):196.
[5] Levine R.(1991) Recognized and possible effects of pesticides in hu-mans. In:Hayes WJ,Lawa ER,editor.Handbook of pesticides toxicology, vol.1.Academic Press,New York,20-30.
[6] 方晓航,仇荣亮.有机磷农药在土壤环境中的降解转化[J].环境科学技术,2003,26(2):57.
[7] 李本昌.农药残留量实用检测方法手册(第一卷)[M].北京:中国农业科技出版社,1995:10-15.
[8] 李本昌.农药残留量实用检测方法手册(第二卷)[M].北京:化学工业出版社,2001:20-23.
[9] Sun F,Wong SS,Li GC,Chen SN.(2005)A preliminary assess ment of consumer's exposure to pesticide residues in fisheries products. Chemosphere,57,112.
[10] Covaci A,Gheorghe A, Schepens P.(2004) Distribution of organochlorine pesticides, polychlorinated biphenyls and alpha-HCH enantiomers in pork tissues. Chemosphere, 56,757-766.
[11] R.Doong,C.Lee.(1999)Determination of organochlorine pesticide residues in foods using solid-phase extraction clean -up cartridges. Analyst,124,1287-1289.
[12] Pagliuca G,Gazzotti T,Zironi E, Sticca P. J. (2005)Residue analysis of organophosphorus pesticides in animal matrices by dual column capillary gas chromatography with nitrogen-phospho-rus detection.Chromatogr.A,1071,67-70.
[13] R.K. Juhler.(1998) Supercritical fluid extraction of pesticides from meat:a systematic approach for optimisation. Analyst,123,1551-1556.
[14] R.K.Juhler.(1997)Optimized method for the determi nation of organophosphorus pesticides in meat and fatty matrices.J.Chromatogr.A,786,45-53.
[15] M.S.S.Curren,J.W.(2001)King.Ethanol-modified subcri tical water extraction combined with solid-phase microextra ction for determining atrazine in beef kidney. J. Agric. Food Chem.,49,2175-2180.
[16] C.Soler,J. Ma˜nés, Y. Picó. (2005) Comparison of liquid chromatography using triple quadrupole and quadrupole ion trap mass analyzers to determine pesticide residues in oranges.J.Chromatogr.A,1067,115-125.
[17] Garrido Frenich A, Plaza-Bolaños P, Martínez Vidal JL. (2008) Comparison of tandem-in-space and tandem-in-time mass spectrometry in gas chromatography determination of pesticides: application to simple and complex food samples. J Chromatogr A,1203,229-238.
[18] A.Garrido Frenich,J.L.Fernández Moreno,J.L. Martínez Vidal,F.J.Arrebola Liébanas.(2007)Application of gas chromato graphy coupled to triple quadrupole mass spectrometry for the multiresidue analysis of pesticides in olive oil. J. Agric.Food Chem.,55,8346-8352.
[19] A.Garrido Frenich,P. Plaza Bola˜nos,J.L. (2007)Martínez Vidal. Application of gas chromatography-triple quadrupole mass spectrometry in the quantification-confirmation of pesticides and polychlorinated biphenyls in eggs at trace levels.J.Chromatogr.A,,1167,9-17.
[20] C.Díez,W.A.Traag,P.Zommer,P.(2006)Marinero,J.Atienza.Comparison of an acetonitrile extraction/partitioning and "dispersive solid-phase extraction" method with classical multi-residue methods for the extraction of herbicide residues in barley samples.J.Chromatogr.A,,1131,11-23.
[21] ARomera-Torres A,Arrebola-Liébanas J,Vidal JLM,Fre nich AG.(2019) Determination of Calystegines in Several Tomato Varieties Based on GC-Q-Orbitrap Analysis and Their Classification by ANOVA. J Agric Food Chem,,67,1284-1291.
[22] Martínez Vidal JL, Arrebola Liébanas FJ, González Rodríguez MJ, Garrido Frenich A, Fernández Moreno JL.(2006)Validation of a gas chromatography/triple quadrupole mass spectrometry based method for the quantification of pestic ides in food commodities. Rapid Commun Mass Spectrom,, 20,365-375.
[23] Garrido Frenich A,Plaza-Bolaños P,Martínez Vidal JL.(2008)Comparison of tandem-in-space and tandem-in-time mass spectrometry in gas chromatography determination of pesticides:application to simple and complex food samples. J. Chromatogr.A,,1203,229-238.
[24] Bolaños PP, Frenich AG, Vidal JL.(2005) Application of gas chromatography-triple quadrupole mass spectrometry in the quantification-confirmation of pesticides and polychlo rinated biphenyls in eggs at trace levels.J Chromatogr A,,1167,9-17.
[25] Bolaños PP, Moreno JL, Shtereva DD, Frenich AG, Vidal JL.(2007) Development and validation of a multiresidue method for the analysis of 151 pesticide residues in strawberry by gas chromatography coupled to a triple quadrupole mass analyzer. Rapid Commun Mass Spectrom,21,2282-2294.
[26] Garrido Frenich A, González-Rodríguez MJ, Arrebola FJ,Martínez Vidal JL.(2005)Potentiality of gas chromatography -triple quadrupole mass spectrometry in vanguard and reargu ard methods of pesticide residues in vegetables. Anal Chem.,77,4640-4648
[27] Fernández Moreno JL,Garrido Frenich A,Plaza Bolaños P,Martínez Vidal JL.(2008)Multiresidue method for the analys is of more than 140 pesticide residues in fruits and vegeta bles by gas chromatography coupled to triple quadrupole mass spectrometry. J Mass Spectrom ,43,1235-1254.
[28] J.L.Martínez Vidal,J.L.Fernández Moreno,F.J.A.Liéban as,A.Garrido Frenich. (2007) Application of low-pressure gas chromatography/tandem mass spectrometry to the determinat ion of pesticide residues in tropical fruits.J AOAC Int,,90,1146-1164.
[29] J.L.Fernández Moreno,F.J.Arrebola Liébanas,A.Garrido Frenich, J.L. Martínez Vidal. (2006)Evaluation of different sample treatments for determining pesticide residues in fat vegetable matrices like avocado by low-pressure gas chroma tography-tandem mass spectrometry.J.Chromatogr.A,,1111,97-105.
[30] 祝立群.有机磷农药残留物的GC/MS、GC/MS/MS分析[J].现代科学仪器,1999,15(5): 44-45.
[31] 谢振伟.串联四极杆质谱(GC-QqQ-MS/MS)测定土壤中的有机氯农药和多氯联苯[J].中国环境监测,2008,29(5):20-24.
[32] 杨坪,廖激.浅谈串联四极杆质谱(GC-QqQ-MS/MS)在土壤样品有机污染物分析中的应用[J].四川环境,2008,29(2):5-10.
[33] 蒋雯菁,谢振伟,但德忠.地表水中的有机氯农药和多氯联苯分析研究进展[J].现代科学仪器,2015,20(5):26-33.
[34] 蒋雯菁.地表水中24种有机氯农药和19种多氯联苯的自动SPE-GC-MS/MS分析[J].环境化学,2012, 31(9):1458-1459.
[35] 蒋雯菁,谢振伟.地表水中15种硝基苯类化合物的自动SPE-GC-MS/MS分析研究[J].绿色科技,2022,24(12):99-101.
[36] 董素静.气相色谱/三重四级杆质谱法同时测定蔬菜水果中13种农药残留[J].现代农业科技,2017,45(5):108-110.
[37] 彭汝林,曾婷,朱雨田,等.QuEChERS结合气相色谱-串联三重四极杆质谱快速测定水产品中100种农药残留[J].食品科技,2023,48(8):278-286.
[38] 尚德军,魏帅,李世雨.气相色谱法/三重四极杆质谱测定番茄酱中72种农药残留量[J].食品科学,2013,34(12):237-242.
[39] 陈其煌,朱曼洁,黄和勇,等.气相色谱-离子阱-多级质谱法(GC-IT-MSn)法测定水中22种有机氯和拟除虫菊酯农药残留[J].环境化学,2012,31(10):1665-1666.
[40] 张伟国.气相色谱/离子阱质谱-选择离子方法同时检测大米中百种农药残留[J].分析化学,2006,34(4):484-488.
[41] 郭婕,张燕,,胡振国,等.环境水样中农药污染分析技术研究进展[J].岩矿测试,2021,40(1):16-32.
[42] 杨细蒙,黄茜,郑慧欣,等.高分辨质谱技术在农药残留分析中的应用研究进展[J].北方农业学报,2023,51(1):85-92.
[43] 谢昊臻,胡婷婷,王佳慧,等.基于高分辨质谱技术的植物源性药食同源特色农产品中10种农药残留的测定和快速筛查[J].化学试剂,2022,44(2):266-272.
[44] 刘海灵,王海鹤.四极杆飞行时间串联质谱及其应用[J].现代仪器,2011,17(1):27-29.
[45] 徐江艳,施瑛,高贝贝,等.QuEChERS-高效液相色谱-串联四极杆飞行时间质谱法同时测定大米中7种除草剂残留[J].农药学学报,2019,21(4):468-474.
[46] 陈锦杭,冯城婷,林秋凤,等.Quenchers-固相萃取-气相色谱/四极杆飞行时间质谱法快速测定牛奶中的11种有机磷[J].中国乳品工业,2021,49 (1):51-54.
[47] 姚劲挺,冀峰,郝红元,等.离子阱飞行时间串联质谱快速筛查农产品中农药残留[J].检验检疫学刊,2009,19(5):12-17.
[48] 孙碧霞,郭德华,丁卓平,等.液相色谱-离子阱-飞行时间串联质谱快速筛查蔬菜中188种农药残留[J].分析测试学报,2010,29(10):1017-1024.
[49] 黄晓,田琴琴,范荣荣,等.线性离子阱飞行时间质谱仪的研制及性能表征[J].分析测试学报,2018,37(11):1322-1327.
[50] 李重九.色谱-质谱联用技术的进步与农药多残留分析方法的发展(之二)——从低分辨质谱技术的选择性谈起[J].质谱学报,2021,42(05):681-690.
[51] 盛龙生.有机质谱法及其应用[M].北京: 化学工业出版社,2016.
[2] 李忠民,赵协萍.有机氯农药污染环境与人体的调查分析[J]环境保护,1997,24(8):40-4l.
[3] Dickerson AS,Wu AC,Liew Z,Weisskopf M.(2020)A Scoping Review of Non-Occupation-al Exposures to Environmental Poll utants and Adult Depression, Anxiety, and Suicide. Curr Envi ron Health Rep,7,256-271.
[4] 孔祥虹.固相微萃取-气相色谱法测定浓缩汁中的8种有机磷农药残留[J].食品科学,2009,30(2):196.
[5] Levine R.(1991) Recognized and possible effects of pesticides in hu-mans. In:Hayes WJ,Lawa ER,editor.Handbook of pesticides toxicology, vol.1.Academic Press,New York,20-30.
[6] 方晓航,仇荣亮.有机磷农药在土壤环境中的降解转化[J].环境科学技术,2003,26(2):57.
[7] 李本昌.农药残留量实用检测方法手册(第一卷)[M].北京:中国农业科技出版社,1995:10-15.
[8] 李本昌.农药残留量实用检测方法手册(第二卷)[M].北京:化学工业出版社,2001:20-23.
[9] Sun F,Wong SS,Li GC,Chen SN.(2005)A preliminary assess ment of consumer's exposure to pesticide residues in fisheries products. Chemosphere,57,112.
[10] Covaci A,Gheorghe A, Schepens P.(2004) Distribution of organochlorine pesticides, polychlorinated biphenyls and alpha-HCH enantiomers in pork tissues. Chemosphere, 56,757-766.
[11] R.Doong,C.Lee.(1999)Determination of organochlorine pesticide residues in foods using solid-phase extraction clean -up cartridges. Analyst,124,1287-1289.
[12] Pagliuca G,Gazzotti T,Zironi E, Sticca P. J. (2005)Residue analysis of organophosphorus pesticides in animal matrices by dual column capillary gas chromatography with nitrogen-phospho-rus detection.Chromatogr.A,1071,67-70.
[13] R.K. Juhler.(1998) Supercritical fluid extraction of pesticides from meat:a systematic approach for optimisation. Analyst,123,1551-1556.
[14] R.K.Juhler.(1997)Optimized method for the determi nation of organophosphorus pesticides in meat and fatty matrices.J.Chromatogr.A,786,45-53.
[15] M.S.S.Curren,J.W.(2001)King.Ethanol-modified subcri tical water extraction combined with solid-phase microextra ction for determining atrazine in beef kidney. J. Agric. Food Chem.,49,2175-2180.
[16] C.Soler,J. Ma˜nés, Y. Picó. (2005) Comparison of liquid chromatography using triple quadrupole and quadrupole ion trap mass analyzers to determine pesticide residues in oranges.J.Chromatogr.A,1067,115-125.
[17] Garrido Frenich A, Plaza-Bolaños P, Martínez Vidal JL. (2008) Comparison of tandem-in-space and tandem-in-time mass spectrometry in gas chromatography determination of pesticides: application to simple and complex food samples. J Chromatogr A,1203,229-238.
[18] A.Garrido Frenich,J.L.Fernández Moreno,J.L. Martínez Vidal,F.J.Arrebola Liébanas.(2007)Application of gas chromato graphy coupled to triple quadrupole mass spectrometry for the multiresidue analysis of pesticides in olive oil. J. Agric.Food Chem.,55,8346-8352.
[19] A.Garrido Frenich,P. Plaza Bola˜nos,J.L. (2007)Martínez Vidal. Application of gas chromatography-triple quadrupole mass spectrometry in the quantification-confirmation of pesticides and polychlorinated biphenyls in eggs at trace levels.J.Chromatogr.A,,1167,9-17.
[20] C.Díez,W.A.Traag,P.Zommer,P.(2006)Marinero,J.Atienza.Comparison of an acetonitrile extraction/partitioning and "dispersive solid-phase extraction" method with classical multi-residue methods for the extraction of herbicide residues in barley samples.J.Chromatogr.A,,1131,11-23.
[21] ARomera-Torres A,Arrebola-Liébanas J,Vidal JLM,Fre nich AG.(2019) Determination of Calystegines in Several Tomato Varieties Based on GC-Q-Orbitrap Analysis and Their Classification by ANOVA. J Agric Food Chem,,67,1284-1291.
[22] Martínez Vidal JL, Arrebola Liébanas FJ, González Rodríguez MJ, Garrido Frenich A, Fernández Moreno JL.(2006)Validation of a gas chromatography/triple quadrupole mass spectrometry based method for the quantification of pestic ides in food commodities. Rapid Commun Mass Spectrom,, 20,365-375.
[23] Garrido Frenich A,Plaza-Bolaños P,Martínez Vidal JL.(2008)Comparison of tandem-in-space and tandem-in-time mass spectrometry in gas chromatography determination of pesticides:application to simple and complex food samples. J. Chromatogr.A,,1203,229-238.
[24] Bolaños PP, Frenich AG, Vidal JL.(2005) Application of gas chromatography-triple quadrupole mass spectrometry in the quantification-confirmation of pesticides and polychlo rinated biphenyls in eggs at trace levels.J Chromatogr A,,1167,9-17.
[25] Bolaños PP, Moreno JL, Shtereva DD, Frenich AG, Vidal JL.(2007) Development and validation of a multiresidue method for the analysis of 151 pesticide residues in strawberry by gas chromatography coupled to a triple quadrupole mass analyzer. Rapid Commun Mass Spectrom,21,2282-2294.
[26] Garrido Frenich A, González-Rodríguez MJ, Arrebola FJ,Martínez Vidal JL.(2005)Potentiality of gas chromatography -triple quadrupole mass spectrometry in vanguard and reargu ard methods of pesticide residues in vegetables. Anal Chem.,77,4640-4648
[27] Fernández Moreno JL,Garrido Frenich A,Plaza Bolaños P,Martínez Vidal JL.(2008)Multiresidue method for the analys is of more than 140 pesticide residues in fruits and vegeta bles by gas chromatography coupled to triple quadrupole mass spectrometry. J Mass Spectrom ,43,1235-1254.
[28] J.L.Martínez Vidal,J.L.Fernández Moreno,F.J.A.Liéban as,A.Garrido Frenich. (2007) Application of low-pressure gas chromatography/tandem mass spectrometry to the determinat ion of pesticide residues in tropical fruits.J AOAC Int,,90,1146-1164.
[29] J.L.Fernández Moreno,F.J.Arrebola Liébanas,A.Garrido Frenich, J.L. Martínez Vidal. (2006)Evaluation of different sample treatments for determining pesticide residues in fat vegetable matrices like avocado by low-pressure gas chroma tography-tandem mass spectrometry.J.Chromatogr.A,,1111,97-105.
[30] 祝立群.有机磷农药残留物的GC/MS、GC/MS/MS分析[J].现代科学仪器,1999,15(5): 44-45.
[31] 谢振伟.串联四极杆质谱(GC-QqQ-MS/MS)测定土壤中的有机氯农药和多氯联苯[J].中国环境监测,2008,29(5):20-24.
[32] 杨坪,廖激.浅谈串联四极杆质谱(GC-QqQ-MS/MS)在土壤样品有机污染物分析中的应用[J].四川环境,2008,29(2):5-10.
[33] 蒋雯菁,谢振伟,但德忠.地表水中的有机氯农药和多氯联苯分析研究进展[J].现代科学仪器,2015,20(5):26-33.
[34] 蒋雯菁.地表水中24种有机氯农药和19种多氯联苯的自动SPE-GC-MS/MS分析[J].环境化学,2012, 31(9):1458-1459.
[35] 蒋雯菁,谢振伟.地表水中15种硝基苯类化合物的自动SPE-GC-MS/MS分析研究[J].绿色科技,2022,24(12):99-101.
[36] 董素静.气相色谱/三重四级杆质谱法同时测定蔬菜水果中13种农药残留[J].现代农业科技,2017,45(5):108-110.
[37] 彭汝林,曾婷,朱雨田,等.QuEChERS结合气相色谱-串联三重四极杆质谱快速测定水产品中100种农药残留[J].食品科技,2023,48(8):278-286.
[38] 尚德军,魏帅,李世雨.气相色谱法/三重四极杆质谱测定番茄酱中72种农药残留量[J].食品科学,2013,34(12):237-242.
[39] 陈其煌,朱曼洁,黄和勇,等.气相色谱-离子阱-多级质谱法(GC-IT-MSn)法测定水中22种有机氯和拟除虫菊酯农药残留[J].环境化学,2012,31(10):1665-1666.
[40] 张伟国.气相色谱/离子阱质谱-选择离子方法同时检测大米中百种农药残留[J].分析化学,2006,34(4):484-488.
[41] 郭婕,张燕,,胡振国,等.环境水样中农药污染分析技术研究进展[J].岩矿测试,2021,40(1):16-32.
[42] 杨细蒙,黄茜,郑慧欣,等.高分辨质谱技术在农药残留分析中的应用研究进展[J].北方农业学报,2023,51(1):85-92.
[43] 谢昊臻,胡婷婷,王佳慧,等.基于高分辨质谱技术的植物源性药食同源特色农产品中10种农药残留的测定和快速筛查[J].化学试剂,2022,44(2):266-272.
[44] 刘海灵,王海鹤.四极杆飞行时间串联质谱及其应用[J].现代仪器,2011,17(1):27-29.
[45] 徐江艳,施瑛,高贝贝,等.QuEChERS-高效液相色谱-串联四极杆飞行时间质谱法同时测定大米中7种除草剂残留[J].农药学学报,2019,21(4):468-474.
[46] 陈锦杭,冯城婷,林秋凤,等.Quenchers-固相萃取-气相色谱/四极杆飞行时间质谱法快速测定牛奶中的11种有机磷[J].中国乳品工业,2021,49 (1):51-54.
[47] 姚劲挺,冀峰,郝红元,等.离子阱飞行时间串联质谱快速筛查农产品中农药残留[J].检验检疫学刊,2009,19(5):12-17.
[48] 孙碧霞,郭德华,丁卓平,等.液相色谱-离子阱-飞行时间串联质谱快速筛查蔬菜中188种农药残留[J].分析测试学报,2010,29(10):1017-1024.
[49] 黄晓,田琴琴,范荣荣,等.线性离子阱飞行时间质谱仪的研制及性能表征[J].分析测试学报,2018,37(11):1322-1327.
[50] 李重九.色谱-质谱联用技术的进步与农药多残留分析方法的发展(之二)——从低分辨质谱技术的选择性谈起[J].质谱学报,2021,42(05):681-690.
[51] 盛龙生.有机质谱法及其应用[M].北京: 化学工业出版社,2016.
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